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: concentration profile analysis by Secondary Ion Mass Spectrometry (SIMS), transmission electron microscopy (TEM), Raman spectroscopy, and X-ray absorption spectroscopy. This thesis is part of the European FIGARO
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. The primary goal of this thesis is to develop innovative methodology that bridges Ultrafast Transmission Electron Microscopy (UTEM) and environmental TEM using in situ gas-heating holders. Once realized, this
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, 2028 730 days Advanced microstructural characterization: Operation and analysis using advanced analytical techniques (GISAXS, GIWAXS, TEM, SCLC experiments) to correlate the evolution
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, and a 100 keV Tundra cryo-TEM. We have regular access to the 22-ID beamline at the Argonne Photon Source for X-ray data collection, as well as to a Titan Krios microscope equipped with a Gatan K3 camera
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of the microstructure, possibility of one step synthesis / shaping of the SSE membrane while ensuring scalability and low cost. The produced materials will be characterized by XRD and SEM/TEM, and used to prepare Solid
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, numerical process simulation, and advanced characterization techniques (synchrotron, TEM, EBSD), will be implemented. The ideal candidate will hold a Master's degree or an engineering degree in Materials
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conditions at UoM experimental facilities: using EBSD and TEM to investigate phase stability, grain structure, and potential cryogenic-induced microstructural evolution, and Tensile testing to evaluate
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). - Experience in metal (for exemple Cu) nanoparticle deposition methods - Strong knowledge in materials characterizations (XRD, Gaz physisorption, SEM, TEM, XPS, UV-Vis spectrometry) - Additional knowledge in gas
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physics, chemistry, biology and soft matter. We perform systematic characterization using complementary techniques, including cutting-edge TEM methods such as electron ptychography and holography, enabling
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with EDS, EBSD, TEM, and XRD, available either on-site or within the Slovak Academy of Sciences. Process and physical modelling will be performed using freely available scientific software such as Octave